HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,5-Dibenzyl-2,5-diazabicyclo[2.2.2]octane-3,6-dione → 2,5-Dibenzyl-2,5-diazabicyclo[2.2.2]octane
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,5-Dibenzyl-2,5-diazabicyclo[2.2.2]octane-3,6-dione | HCID 21545490 | — |
| Reactant | 8-Benzyl-3-methyl-3,8-diazabicyclo[3.2.1]octane | HCID 21545507 | — |
| Product | 2,5-Dibenzyl-2,5-diazabicyclo[2.2.2]octane | HCID 21545495 | 88.2% |
Reaction Steps
Reduction of 6.1 g (0.019 mole) of 2.5-dibenzyl-2,5-diazabicyclo[2.2.2]octane-3,6-dione by the procedure employed to prepare 8-benzyl-3-methyl-3,8-diazabicyclo[3.2.1]octane as related under Example 5 gave 4.9 g (88%) of 2,5-dibenzyl-2,5-diazabicyclo[2.2.2]octane as a colorless oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03951980 |
| Source dataset | uspto-grants-1976_04 |
| ORD ID | ord-935699de279a40c485bc3c5a131dc5de |
| Source note | uspto-grants-1976_04 |