HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diethyl Ether → HCID 12201360, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diethyl Ether | HCID 3283 | — |
| Reactant | Diazomethane | HCID 9550 | — |
| Reactant | 2,3-Dichloro-1,4-benzoquinone | HCID 138423 | — |
| Product | HCID 12201360 | HCID 12201360 | — |
Reaction Steps
2,3-Dichlorobenzoquinone (22 grams) was added portionwise to a stirred solution of diazomethane (14 grams) in ether (500 milliliters) maintained at a temperature below 15° C. A pale yellow solid separated out from the solution, and this was filtered off and dried to yield the desired product having a melting point of 176°-177° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03952003 |
| Source dataset | uspto-grants-1976_04 |
| ORD ID | ord-adbe37ebfb0d4cee85319ebe0fa69086 |
| Source note | uspto-grants-1976_04 |