HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydroxyamine hydrochloride → HCID 136227082, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydroxyamine hydrochloride | HCID 443297 | — |
| Reactant | (4-Ethyl-2-hydroxyphenyl)(4-fluorophenyl)methanone | HCID 12562657 | — |
| Product | HCID 136227082 | HCID 136227082 | — |
Reaction Steps
4-Ethyl-4'-fluoro-2-hydroxybenzophenone (21.0g, 80% pure) was treated with hydroxylamine hydrochloride (24.0g) similarly to Example 12, to give, after recrystallisation from benzene, the title compound as a white crystalline solid (10.7g), m.p. 130°-2°C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03951999 |
| Source dataset | uspto-grants-1976_04 |
| ORD ID | ord-3e74400b71e84ba2a3b77e5a62bc0b9f |
| Source note | uspto-grants-1976_04 |