HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzene → (3-Ethyl-2-hydroxyphenyl)(phenyl)methanone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzene | HCID 241 | — |
| Reactant | 3-Ethyl-2-hydroxybenzoyl chloride | HCID 45081581 | — |
| Product | (3-Ethyl-2-hydroxyphenyl)(phenyl)methanone | HCID 12562658 | 58.1% |
Reaction Steps
This compound (44.67g) was prepared from benzene (172g.,2.2 mole) and 2-hydroxy-3-ethyl benzoic acid chloride (63.15g,0.34 mole), using the same conditions as in Example 30. The b.p. of the compound was 123°-126°C./0.14mm, ηD22 1.6081,νmax.(film) 1630cm-1.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03951999 |
| Source dataset | uspto-grants-1976_04 |
| ORD ID | ord-ffda8fb0273d4c46a235d9c7a3e268e0 |
| Source note | uspto-grants-1976_04 |