Acetyl chloride → HCID 54441192, compound

HRID 1606030Notes

Reaction equation

HRID 1606030 reaction equation
[N+:1]([C:4]1[N:8]([CH2:9][CH2:10][OH:11])[C:7]([CH:12]=[CH:13][N:14]([CH3:16])[CH3:15])=[N:6][CH:5]=1)([O-:3])=[O:2].[C:17](Cl)(=[O:19])[CH3:18]>>[N+:1]([C:4]1[N:8]([CH2:9][CH2:10][O:11][C:17](=[O:19])[CH3:18])[C:7]([CH:12]=[CH:13][N:14]([CH3:15])[CH3:16])=[N:6][CH:5]=1)([O-:3])=[O:2]

Participants

3

Reactant 2

HCID 6367Acetyl chlorideHCID 54304831HCID 54304831, compound

Product 1

HCID 54441192HCID 54441192, compound

Procedure

2,26 g. (0.01 mole) of 5-nitro-1-(2-hydroxyethyl)-2-(2-dimethylaminovinyl)-imidazole and 0.79 g. (0.01 mole) of acetyl chloride were reacted as described in Example 11. After pouring the reaction mixture on ice water, it was extracted with chloroform and the chloroform solution evaporated. The crude red oil exhibited the characteristic UV maxima in methanol:

Workup

  1. additionAfter pouring the reaction mixture on ice water, it
  2. extractionwas extracted with chloroform
  3. customthe chloroform solution evaporated

Sources & evidence

ORD record
ord-1afb53654eb543b5b50816c1f7fc50b5
Source dataset
uspto-grants-1976_04
Patent number
US03952007

Reaction notes

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