Dipropylcarbamoyl chloride → 1-Dipropylcarbamoyl-3-ethylsulphonyl-1,2,4-triazole

HRID 1606069Notes

Reaction equation

[CH2:1]([S:3]([C:6]1[N:10]=[CH:9][NH:8][N:7]=1)(=[O:5])=[O:4])[CH3:2].[CH2:11]([N:14]([CH2:18][CH2:19][CH3:20])[C:15](Cl)=[O:16])[CH2:12][CH3:13]>>[CH2:11]([N:14]([CH2:18][CH2:19][CH3:20])[C:15]([N:8]1[CH:9]=[N:10][C:6]([S:3]([CH2:1][CH3:2])(=[O:5])=[O:4])=[N:7]1)=[O:16])[CH2:12][CH3:13]

Participants

Reactant 2

HCID 3015348Dipropylcarbamoyl chloride

HCID 178477666HCID 178477666, compound

Product 1

HCID 203549621-Dipropylcarbamoyl-3-ethylsulphonyl-1,2,4-triazole

Procedure

In an analogous manner to that described in Example 20, 3-ethylsulphonyl-1,2,4-triazole was reacted with dipropylcarbamoyl chloride to give 1-dipropylcarbamoyl-3-ethylsulphonyl-1,2,4-triazole, m.p. 44° - 45°C. Elemental analysis satisfactory.

Sources & evidence

ORD record: ord-21c855566427467a94ed5679c820f674
Source dataset: uspto-grants-1976_04
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US03952001

Reaction notes

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