Acetyl chloride → Furfuryl thioacetate

HRID 1606197Notes

Reaction equation

[C:1](Cl)(=[O:3])[CH3:2].[CH2:5]([SH:11])[C:6]1[O:10][CH:9]=[CH:8][CH:7]=1>>[CH3:2][C:1]([S:11][CH2:5][C:6]1[O:10][CH:9]=[CH:8][CH:7]=1)=[O:3]

Participants

Reactant 2

HCID 6367Acetyl chloride

HCID 73632-Furanmethanethiol

Product 1

HCID 61660Furfuryl thioacetate

Procedure

Furfurylthiol acetate was prepared by reacting acetic chloride or anhydride with furfurylmercaptan according to the method described in Houben-Weyl, 4th ed., vol. 9, 753 (1955). The product has a b.p. of 90°-92°C./12 mm. Hg.

Sources & evidence

ORD record: ord-551b854a4bcc471c83b3185e1b34a854
Source dataset: uspto-grants-1976_04
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US03952024

Reaction notes

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