HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Methylbutanal → HCID 54495141, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Methylbutanal | HCID 11552 | — |
| Reactant | 4-Methylthiazole | HCID 12748 | — |
| Reactant | Lithium | HCID 3028194 | — |
| Reactant | Butyllithium | HCID 178418339 | — |
| Product | HCID 54495141 | HCID 54495141 | — |
Reaction Steps
d. Isobutyl (4-methyl-2-thiazolyl) carbinol was prepared by starting from 4-methyl-thiazole and substituting the hydrogen atom in the 2-position by lithium by reaction with butyl-lithium. The resulting metal-organic compound was reacted with isovaleraldehyde [cf. J.A.C.S. 74, 6260 (1952)]. The resulting product had a b.p. of 94° C/0.1 mm. Hg.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03952026 |
| Source dataset | uspto-grants-1976_04 |
| ORD ID | ord-091b29fa55c7402da570d1c821b9c74d |
| Source note | uspto-grants-1976_04 |