Methyl iodide → HCID 86733269, compound

HRID 1606265Notes

Reaction equation

HRID 1606265 reaction equation
[CH:1]([N:4]=[C:5]1[CH:9]2[CH2:10][C:11]3[CH:12]=[CH:13][CH:14]=[CH:15][C:16]=3[CH:8]2[CH2:7][CH2:6]1)([CH3:3])[CH3:2].[CH3:17][I:18]>>[I-:18].[C:5]1(=[N+:4]([CH:1]([CH3:3])[CH3:2])[CH3:17])[CH:9]2[CH2:10][C:11]3[CH:12]=[CH:13][CH:14]=[CH:15][C:16]=3[CH:8]2[CH2:7][CH2:6]1

Participants

3

Reactant 2

HCID 6328Methyl iodideHCID 21546245HCID 21546245, compound

Product 1

HCID 86733269HCID 86733269, compound

Procedure

3,3a,8,8a-Tetrahydro-N-isopropylcyclopent[a]inden-1[2H]-imine (1.4 g) and methyl iodide (3 ml) were kept at room temperature overnight. The resultant solid mass was triturated with ether to give the quaternary salt as a buff solid, m.p. 168°-170°.

Workup

  1. customThe resultant solid mass was triturated with ether
  2. customto give the quaternary salt as a buff solid, m.p. 168°-170°

Sources & evidence

ORD record
ord-12c7d97046304d29967991ba141a3053
Source dataset
uspto-grants-1976_04
Patent number
US03952050

Reaction notes

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