HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → 1175-97-9
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | Ampicillin Trihydrate | HCID 23565 | — |
| Reactant | Sulfuric acid magnesium salt (1:1) | HCID 24083 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | 1175-97-9 | HCID 12918994 | — |
Reaction Steps
After stirring a mixture of 12 g. of ampicillin trihydrate, 9 g. of anhydrous magnesium sulfate, 8.4 ml. of triethylamine, and 190 ml. of dichloromethane for 1 hour at room temperature, the magnesium sulfate was filtered away to provide dichloromethane solution of ampicillin triethylamine salt.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03953428 |
| Source dataset | uspto-grants-1976_04 |
| ORD ID | ord-89d47fffae0c431894d00844f5c02508 |
| Source note | uspto-grants-1976_04 |