HuagongsheHuagongshe Chemistry Print Report · For research reference only
Nitroethane → HCID 53815307, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Nitroethane | HCID 6587 | — |
| Reactant | Ammonium Acetate | HCID 517165 | — |
| Reactant | 5-chloro-1H-indole-3-carbaldehyde | HCID 2795374 | — |
| Product | HCID 53815307 | HCID 53815307 | — |
Reaction Steps
12.9 g of 5-chloro-3-formylindole and 1.3 g of ammonium acetate are suspended in 26 ml of nitroethane and refluxed for 1 hour. After the whole of the reactants have dissolved a mass of orange crystals are seen to form. The reaction mixture is then cooled and filtered after dilution with di-isopropyl ether. The product is recrystallised from 96% ethyl alcohol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03953442 |
| Source dataset | uspto-grants-1976_04 |
| ORD ID | ord-1e06bd887ebb416a9775cb88260288df |
| Source note | uspto-grants-1976_04 |