HCID 20498440, compound → HCID 14669074, compound

HRID 1606528Notes

Reaction equation

HRID 1606528 reaction equation
Br.[NH2:2][C:3]1[N:7]2[C:8]3[C:13]([CH:14]=[CH:15][C:6]2=[N:5][N:4]=1)=[CH:12][CH:11]=[CH:10][CH:9]=3.C([O-])(=O)C.[Na+].[OH-].[Na+]>O>[NH2:2][C:3]1[N:7]2[C:8]3[C:13]([CH:14]=[CH:15][C:6]2=[N:5][N:4]=1)=[CH:12][CH:11]=[CH:10][CH:9]=3

Participants

4

Reactant 2

HCID 20498440HCID 20498440, compoundHCID 21543672HCID 21543672, compound

Product 1

HCID 14669074HCID 14669074, compound

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

The 1-amino-s-triazolo(4,3-a)quinoline hydrobromide obtained as reported in the preceding example was dissolved in water. A sodium acetate/sodium hydroxide mixture was added to break up the salt. The product then precipitated out as the free base, m.p., 250°-3°C.

Workup

  1. customThe product then precipitated out as the free base, m.p., 250°-3°C.

Sources & evidence

ORD record
ord-6ccfd99b411341e18183716926f03745
Source dataset
uspto-grants-1976_04
Patent number
US03953457

Reaction notes

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