HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Cyano-2-ethoxy-2-methylaminoethylene → HCID 178483853, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Cyano-2-ethoxy-2-methylaminoethylene | HCID 73683202 | — |
| Reactant | HCID 178433288 | HCID 178433288 | — |
| Product | HCID 178483853 | HCID 178483853 | — |
Reaction Steps
4-Methyl-5-[(2-aminoethyl)thiomethyl]imidazole (3.5g) was added to a solution of 1-cyano-2-ethoxy-2-methylaminoethylene (3.1g) and the solution was stirred for 5 hours at 100°. The product was chromatographed on a column of neutral alumina with elution bychloroform/ethyl acetate (1:1) to give the title compound as a glass.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03953460 |
| Source dataset | uspto-grants-1976_04 |
| ORD ID | ord-dde605242e8b4fdc815d58849b162fa5 |
| Source note | uspto-grants-1976_04 |