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1,1-Dimethylhydrazine → 3-Furfurylamino-4-chloro-5-methylsulfinylbenzoic acid 2,2-diethylhydrazide
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 1,1-Dimethylhydrazine | HCID 5976 | — |
| 反応物 | 1,2-Diethylhydrazine | HCID 15374 | — |
| 反応物 | 2-Butenamide | HCID 5354487 | — |
| 反応物 | N-tert-butyl-3-(3-furfurylamino-4-chloro-5-methylsulfinylbenzoyloxy)crotonamide | HCID 68136665 | — |
| 生成物 | 3-Furfurylamino-4-chloro-5-methylsulfinylbenzoic acid 2,2-diethylhydrazide | HCID 53890761 | — |
反応手順
By replacing the crotonamide and the unsymmetrical-dimethylhydrazine employed in Example 38 by equimolar quantities of N-tert-butyl-3-(3-furfurylamino-4-chloro-5-methylsulfinylbenzoyloxy)crotonamide and unsymmetrical-diethylhydrazine respectively and then following substantially the same procedure described in Example 38 there is obtained 3-furfurylamino-4-chloro-5-methylsulfinylbenzoic acid 2,2-diethylhydrazide.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US03953476 |
| 出典データセット | uspto-grants-1976_04 |
| ORD ID | ord-f0495342c44d4893b56747ec0197063f |
| 出典メモ | uspto-grants-1976_04 |