HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → 2,4-Bis(2-hydroxybenzamido)benzoic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 13066646 | HCID 13066646 | — |
| Product | 2,4-Bis(2-hydroxybenzamido)benzoic acid | HCID 191314 | 85% |
Reaction Steps
By the procedure similar to that described in Example 5, methyl 2,4-bis(2'-acetoxybenzamido)-benzoate obtained in Example 6 was hydrolized with the aid of sodium hydroxide. Recrystallization of the hydrolized product from a mixture of dioxane and water gave 2,4-bis(salicylamido)-benzoic acid having a melting point between 250° - 252°C (decomposition). (Yield; 85%)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03953496 |
| Source dataset | uspto-grants-1976_04 |
| ORD ID | ord-3f8b3b60fef3453497e01aa0e2ce9ffa |
| Source note | uspto-grants-1976_04 |