2,4-Diaminobenzoic acid → HCID 21544118, compound

HRID 1606645Notes

Reaction equation

HRID 1606645 reaction equation
[NH2:1][C:2]1[CH:10]=[C:9]([NH2:11])[CH:8]=[CH:7][C:3]=1[C:4]([OH:6])=[O:5].[CH2:12]([O:14][C:15]1[CH:23]=[CH:22][CH:21]=[CH:20][C:16]=1[C:17](Cl)=[O:18])[CH3:13]>>[CH2:12]([O:14][C:15]1[CH:23]=[CH:22][CH:21]=[CH:20][C:16]=1[C:17]([NH:1][C:2]1[CH:10]=[C:9]([NH:11][C:17](=[O:18])[C:16]2[CH:20]=[CH:21][CH:22]=[CH:23][C:15]=2[O:14][CH2:12][CH3:13])[CH:8]=[CH:7][C:3]=1[C:4]([OH:6])=[O:5])=[O:18])[CH3:13]

Participants

3

Reactant 2

HCID 691342,4-Diaminobenzoic acidHCID 30163972-Ethoxybenzoyl chloride

Product 1

HCID 21544118HCID 21544118, compound

Procedure

By the procedure similar to that described in Example 1, 2,4-diaminobenzoic acid was condensed with 2-ethoxybenzoylchloride to obtain 2,4-bis(2'-ethoxybenzamido)-benzoic acid having a melting point between 225° - 226°C.

Sources & evidence

ORD record
ord-06f2033a071f41419498ccafdd7d80a0
Source dataset
uspto-grants-1976_04
Patent number
US03953496

Reaction notes

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