2-Methoxybenzoyl chloride → HCID 21544115, compound

HRID 1606646Notes

Reaction equation

HRID 1606646 reaction equation
[NH2:1][C:2]1[CH:3]=[C:4]([CH:8]=[C:9]([NH2:11])[CH:10]=1)[C:5]([NH2:7])=[O:6].[CH3:12][O:13][C:14]1[CH:22]=[CH:21][CH:20]=[CH:19][C:15]=1[C:16](Cl)=[O:17]>>[CH3:12][O:13][C:14]1[CH:22]=[CH:21][CH:20]=[CH:19][C:15]=1[C:16]([NH:1][C:2]1[CH:3]=[C:4]([CH:8]=[C:9]([NH:11][C:16](=[O:17])[C:15]2[CH:19]=[CH:20][CH:21]=[CH:22][C:14]=2[O:13][CH3:12])[CH:10]=1)[C:5]([NH2:7])=[O:6])=[O:17]

Participants

3

Reactant 2

HCID 889692-Methoxybenzoyl chlorideHCID 115137753,5-diaminobenzamide

Product 1

HCID 21544115HCID 21544115, compound

Procedure

By the procedure similar to that described in Example 12, 3,5-diaminobenzamide was condensed with 2-methoxybenzoylchloride to obtain 3,5-bis(2'-methoxybenzamido)-benzamide having a melting point between 226° - 227°C.

Sources & evidence

ORD record
ord-2c3baf5bbd7d44c9b895a6ba8ef44e99
Source dataset
uspto-grants-1976_04
Patent number
US03953496

Reaction notes

Loading…