2-Methoxybenzoyl chloride → HCID 54072336, compound

HRID 1606649Notes

Reaction equation

HRID 1606649 reaction equation
[C:1]([O:4][C:5]1[CH:23]=[CH:22][CH:21]=[CH:20][C:6]=1[C:7]([NH:9][C:10]1[CH:18]=[C:17]([NH2:19])[CH:16]=[CH:15][C:11]=1[C:12]([OH:14])=[O:13])=[O:8])(=[O:3])[CH3:2].[CH3:24][O:25][C:26]1[CH:34]=[CH:33][CH:32]=[CH:31][C:27]=1[C:28](Cl)=[O:29]>>[C:1]([O:4][C:5]1[CH:23]=[CH:22][CH:21]=[CH:20][C:6]=1[C:7]([NH:9][C:10]1[CH:18]=[C:17]([NH:19][C:28](=[O:29])[C:27]2[CH:31]=[CH:32][CH:33]=[CH:34][C:26]=2[O:25][CH3:24])[CH:16]=[CH:15][C:11]=1[C:12]([OH:14])=[O:13])=[O:8])(=[O:3])[CH3:2]

Participants

3

Reactant 2

HCID 889692-Methoxybenzoyl chlorideHCID 21544120HCID 21544120, compound

Product 1

HCID 54072336HCID 54072336, compound

Procedure

By the procedure similar to that described in Example 23, 2-(2' -acetoxybenzamido)-4-aminobenzoic acid and 2-methoxybenzoylchloride were allowed to react and were treated to obtain crude crystals. Recrystallization from ethanol gave 2-(2'-acetoxybenzamido)-4-(2'-methoxybenzamido)-benzoic acid having a melting point between 197° - 198°C.

Workup

  1. customto react
  2. additionwere treated
  3. customto obtain crude crystals
  4. customRecrystallization from ethanol

Sources & evidence

ORD record
ord-7060563072dc4ff7a58d3f076e204d9a
Source dataset
uspto-grants-1976_04
Patent number
US03953496

Reaction notes

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