HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Methoxybenzoyl chloride → 2,4-Bis(2-methoxybenzamido)benzoic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Methoxybenzoyl chloride | HCID 88969 | — |
| Reactant | HCID 21544126 | HCID 21544126 | — |
| Product | 2,4-Bis(2-methoxybenzamido)benzoic acid | HCID 13066652 | — |
Reaction Steps
By the procedure similar to that described in Example 23, 2-(2'-methoxybenzamido)-4-aminobenzoic acid and 2-methoxybenzoylchloride were reacted and treated to obtain crude crystals. Recrystallization from aqueous alcohol gave 2,4-bis(2'-methoxybenzamido)-benzoic acid having a melting point between 232° - 233°C which was identical to that obtained in Example 10.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03953496 |
| Source dataset | uspto-grants-1976_04 |
| ORD ID | ord-417836d76dba41538231550f825b3c57 |
| Source note | uspto-grants-1976_04 |