2-Butoxybenzoyl chloride → HCID 21544121, compound

HRID 1606651Notes

Reaction equation

HRID 1606651 reaction equation
[CH2:1]([O:5][C:6]1[CH:26]=[CH:25][CH:24]=[CH:23][C:7]=1[C:8]([NH:10][C:11]1[CH:21]=[C:20]([NH2:22])[CH:19]=[CH:18][C:12]=1[C:13]([O:15][CH2:16][CH3:17])=[O:14])=[O:9])[CH2:2][CH2:3][CH3:4].[CH2:27]([O:31][C:32]1[CH:40]=[CH:39][CH:38]=[CH:37][C:33]=1[C:34](Cl)=[O:35])[CH2:28][CH2:29][CH3:30]>>[CH2:1]([O:5][C:6]1[CH:26]=[CH:25][CH:24]=[CH:23][C:7]=1[C:8]([NH:10][C:11]1[CH:21]=[C:20]([NH:22][C:34](=[O:35])[C:33]2[CH:37]=[CH:38][CH:39]=[CH:40][C:32]=2[O:31][CH2:27][CH2:28][CH2:29][CH3:30])[CH:19]=[CH:18][C:12]=1[C:13]([O:15][CH2:16][CH3:17])=[O:14])=[O:9])[CH2:2][CH2:3][CH3:4]

Participants

3

Reactant 2

HCID 159219152-Butoxybenzoyl chlorideHCID 21544123HCID 21544123, compound

Product 1

HCID 21544121HCID 21544121, compound

Procedure

By the procedure similar to that described in example 21, ethyl 2-(2'-n-butoxybenzamido)-4-aminobenzoate and 2-n-butoxybenzoylchloride were reacted and treated to obtain crude crystals. Recrystallization from ethanol gave ethyl 2,4-bis(2'-n-butoxybenzamido)-benzoate having a melting point between 134° - 136°C.

Workup

  1. customwere reacted
  2. additiontreated
  3. customto obtain crude crystals
  4. customRecrystallization from ethanol

Sources & evidence

ORD record
ord-d7699bb1876e47d080d3affe1788d429
Source dataset
uspto-grants-1976_04
Patent number
US03953496

Reaction notes

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