HCID 54278496, compound → HCID 54419336, compound

Participants

Reaction Steps

By the procedure similar to that described in Example 21, n-butyl 2-(2'-acetoxybenzamido)-4-aminobenzoate and 2'-acetoxybenzoylchloride were reacted and treated to obtain a sticky mass. The mass was dissolved in diethyl ether and a physical stimulus was given to the solution to obtain crystals which precipitated. Recrystallization from ethanol gave n-butyl 2,4-bis(2'-acetoxybenzamido)-benzoate having a melting point between 149° - 152°C.

Provenance & Evidence