2-Methoxybenzoyl chloride → HCID 54452390, compound

HRID 1606653Notes

Reaction equation

HRID 1606653 reaction equation
[NH2:1][C:2]1[CH:10]=[C:9]([NH:11][C:12](=[O:23])[C:13]2[CH:18]=[CH:17][CH:16]=[CH:15][C:14]=2[O:19][C:20](=[O:22])[CH3:21])[CH:8]=[CH:7][C:3]=1[C:4]([OH:6])=[O:5].[CH3:24][O:25][C:26]1[CH:34]=[CH:33][CH:32]=[CH:31][C:27]=1[C:28](Cl)=[O:29]>>[CH3:24][O:25][C:26]1[CH:34]=[CH:33][CH:32]=[CH:31][C:27]=1[C:28]([NH:1][C:2]1[CH:10]=[C:9]([NH:11][C:12](=[O:23])[C:13]2[CH:18]=[CH:17][CH:16]=[CH:15][C:14]=2[O:19][C:20](=[O:22])[CH3:21])[CH:8]=[CH:7][C:3]=1[C:4]([OH:6])=[O:5])=[O:29]

Participants

3

Reactant 2

HCID 889692-Methoxybenzoyl chlorideHCID 21544125HCID 21544125, compound

Product 1

HCID 54452390HCID 54452390, compound

Procedure

By the procedure similar to that described in Example 23, 2-amino-4-(2'-acetoxybenzamido)-benzoic acid and 2-methoxybenzoylchloride were reacted and treated to obtain crude crystals. Recrystallization from water-ethanol gave 2-(2'-methoxybenzamido)-4-(2'-acetoxybenzamido)-benzoic acid which was identical to that of Example 23.

Workup

  1. customwere reacted
  2. additiontreated
  3. customto obtain crude crystals
  4. customRecrystallization from water-ethanol

Sources & evidence

ORD record
ord-d3673b9f438a45b79ea98d55a897069c
Source dataset
uspto-grants-1976_04
Patent number
US03953496

Reaction notes

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