Sodium Hydroxide → HCID 21544595, compound

HRID 1606751Notes

Reaction equation

HRID 1606751 reaction equation
[O:1]=[C:2]1[C:11]2[CH:10]=[CH:9][C:8]3[C:12]4[NH:13][C:14]([C:21]([O:23]C)=[O:22])=[CH:15][C:16](=[O:20])[C:17]=4[CH:18]=[CH:19][C:7]=3[C:6]=2[NH:5][C:4]([C:25]([O:27]C)=[O:26])=[CH:3]1.[OH-].[Na+:30]>O.CO>[O:20]=[C:16]1[C:17]2[CH:18]=[CH:19][C:7]3[C:6]4[NH:5][C:4]([C:25]([O-:27])=[O:26])=[CH:3][C:2](=[O:1])[C:11]=4[CH:10]=[CH:9][C:8]=3[C:12]=2[NH:13][C:14]([C:21]([O-:23])=[O:22])=[CH:15]1.[Na+:30].[Na+:30]

Participants

5

Reactant 2

HCID 14798Sodium HydroxideHCID 12402990HCID 12402990, compound

Product 1

HCID 21544595HCID 21544595, compound

Reagents, catalysts & solvents 2

HCID 887MethanolSolventHCID 962WaterSolvent

Procedure

1.0 gram of the diester prepared in Example 1 is heated in 50 ml. of 1.0N NaOH for 30 minutes. The mixture is cooled, diluted with water, and methanol added. The precipitate is filtered and collected.

Workup

  1. temperatureThe mixture is cooled
  2. additionadded
  3. filtrationThe precipitate is filtered
  4. customcollected

Sources & evidence

ORD record
ord-d179fcd62a4544cea5ed813c2f7f0204
Source dataset
uspto-grants-1976_04
Patent number
US03953598

Reaction notes

Loading…