HCID 21544457, compound → HCID 12282091, compound
Reaction equation
OC[CH2:3][S:4][C:5]1[CH:13]=[CH:12][C:11]([C:14]([F:17])([F:16])[F:15])=[CH:10][C:6]=1[C:7]([OH:9])=[O:8].C(SC1C=CC(C(F)(F)F)=CC=1C(O)=O)C=CC>>[CH3:3][S:4][C:5]1[CH:13]=[CH:12][C:11]([C:14]([F:15])([F:16])[F:17])=[CH:10][C:6]=1[C:7]([OH:9])=[O:8]Participants
3
Procedure
In a similar manner are prepared: 2-(2-hydroxyethylthio)-5-trifluoromethylbenzoic acid, m.p. 153°-154° C.; 2-crotylthio-5-trifluoromethylbenzoic acid, m.p. 139°-141° C.; 2-methallythio-5-trifluoromethylbenzoic acid, m.p. 150°-152° C. and 2-allythio-5-trifluoromethylbenzoic acid, m.p. 178°-190° C.
Workup
- customIn a similar manner are prepared
Sources & evidence
- ORD record
- ord-9d2837c81ca24246aec51524213574c8
- Source dataset
- uspto-grants-1976_04
- Patent number
- US03953595
Reaction notes
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