HuagongsheHuagongshe Chemistry Print Report · For research reference only
N,N-Dimethyltetradecylamine → Phenoxycarbonylmethyltetradecyldimethyl ammonium bromide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N,N-Dimethyltetradecylamine | HCID 8211 | — |
| Reactant | Phenyl Bromoacetate | HCID 564919 | — |
| Product | Phenoxycarbonylmethyltetradecyldimethyl ammonium bromide | HCID 86733359 | — |
Reaction Steps
A mixture of 55 g (0.26 mol) phenyl bromoacetate and 62 g (0.26 mol) of tetradecyldimethylamine was allowed to stand at room temperature for three days. The resultant crystalline mass was washed well with ether and dried to 114 g. Recrystallized from ethyl acetate and vacuum dried, the compound melted at 87°-91.5°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03953605 |
| Source dataset | uspto-grants-1976_04 |
| ORD ID | ord-eb5b6ea58e9a4f4dbd40412f795502a4 |
| Source note | uspto-grants-1976_04 |