HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Ethylphenol → HCID 22749859, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Ethylphenol | HCID 31242 | — |
| Reactant | Sodium | HCID 5360545 | — |
| Reactant | 2,6-Octadiene, 1-bromo-3,7-dimethyl-, (2E)- | HCID 5365867 | — |
| Reactant | 1-[(3,7-Dimethylocta-2,6-dien-1-yl)oxy]-4-ethylbenzene | HCID 54241821 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 22749859 | HCID 22749859 | — |
Reaction Steps
For the synthesis of the two compounds the intermediate, 1-(p-ethylphenoxy)-3,7-dimethyl-2,6-octadiene, was prepared as described by R. E. Redfern et al., Journal of Economic Entomology, 64, 374-376 (1971). The procedure is essentially as follows: The sodium salt of p-ethylphenol was refluxed with geranyl bromide (1-bromo-3,7-dimethyl-2,6-octadiene) in ethanol for several hours to form the p-ethylphenyl geranyl ether which was worked up and distilled in the usual manner; b.p. 122-124/0.06 mm Hg.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03953607 |
| Source dataset | uspto-grants-1976_04 |
| ORD ID | ord-d0360cb8d5c940338e1f4cb11f1a516c |
| Source note | uspto-grants-1976_04 |