HuagongsheHuagongshe Chemistry Print Report · For research reference only
Salicylic Acid → 2-(Dichloromethyl)phenol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Salicylic Acid | HCID 338 | — |
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | Aluminum(III) Chloride | HCID 6451240 | — |
| Product | 2-(Dichloromethyl)phenol | HCID 18008187 | — |
Reaction Steps
A mixture of 10 grams of salicylic acid, 7 ml of thionyl chloride and 0.02 grams of aluminum chloride were heated at 40°-45° C. for 1.5 hours. The excess thionyl chloride was removed in vacuum and salicylyl chloride was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03953596 |
| Source dataset | uspto-grants-1976_04 |
| ORD ID | ord-a460c15847e04d4c8b20d56af5a52bf9 |
| Source note | uspto-grants-1976_04 |