HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Methoxide → HCID 19851157, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Methoxide | HCID 10942334 | — |
| Reactant | 5-Chloro-N1-(2-methoxyethyl)-N3-methyl-2-nitro-1,3-benzenediamine | HCID 19851158 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 19851157 | HCID 19851157 | — |
Reaction Steps
0.019 mole (5 g) of 2-methylamino-6-(β-methoxyethyl)amino-4-chloronitrobenzene was refluxed with 35 ml of 26% sodium methylate in methanol for 45 minutes then diluted with 100 ml of ice water to precipitate the desired product. Following filtering, water washing and drying under vacuum in the presence of P2O5, the product obtained was recrystallized from isopropanol. It melted at 84° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04863482 |
| Source dataset | uspto-grants-1989_09 |
| ORD ID | ord-d58a90feab3246739159828477f4c590 |
| Source note | uspto-grants-1989_09 |