HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Methoxide → HCID 19851159, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Methoxide | HCID 10942334 | — |
| Reactant | HCID 19851165 | HCID 19851165 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 19851159 | HCID 19851159 | — |
Reaction Steps
0.172 mole (40 g) of 2-amino-6-(β-hydroxyethyl)amino-4-chloronitrobenzene in 160 ml of a 30% solution of sodium methylate in methanol was heated for 21/2 hours over a boiling water bath. The desired product precipitated out after dilution with 350 ml of ice water. After recrystallizing from boiling isopropanol to eliminate an insoluble impurity, the desired product melted at 148° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04863482 |
| Source dataset | uspto-grants-1989_09 |
| ORD ID | ord-a9f4c6756bb242529dbe9f7928769561 |
| Source note | uspto-grants-1989_09 |