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HRID1607065

反应详情

EQUATION

反应方程式

HRID 1607065 的结构方程式

REACTANTS

反应物

2
结构：Cc1cc(Br)cnc1CCCCN
HCID13094272

未命名化合物

结构：CSN1Cc2ccccc2S(=O)(=O)N1
HCID19851874

未命名化合物

PRODUCTS

生成物

1
结构：Cc1cc(Br)cnc1CCCCNN1Cc2ccccc2S(=O)(=O)N1
HCID19851867

未命名化合物

PROCEDURE

实验过程

4-(5-Bromo-3-methylpyrid-2-yl)-butylamine (0.73 g) and 3-methylthiobenzothiadiazine-1,1-dioxide (0.68 g) were fused at 130°-140° C. for 3 hours. The product was crystallised from acetonitrile to yield 3-[4-(5-bromo-3-methylpyrid-2-yl)-butylamino]benzothiadiazine-1,1-dioxide m.p. 187°-8° C.

WORKUP

后处理

  1. customThe product was crystallised from acetonitrile