Nitrobenzene → HCID 131716086, compound

HRID 1607066Notes

Reaction equation

[N+](C1C=CC=CC=1)([O-])=[O:2].Br[C:11]1[CH:12]=[C:13]2[C:26]3[CH:16]([CH2:17][C@@H:18]4[C@@H:23]([C:24]=3[CH:25]=1)[CH2:22][C@H:21]([NH:27][C:28](=[O:34])[N:29]([CH2:32][CH3:33])[CH2:30][CH3:31])[CH2:20][N:19]4[CH3:35])[CH2:15][N:14]2[Si](C(C)(C)C)(C)C>>[CH2:32]([N:29]([CH2:30][CH3:31])[C:28]([NH:27][C@H:21]1[CH2:22][C@H:23]2[C@@H:18]([CH2:17][CH:16]3[C:26]4[C:13](=[CH:12][CH:11]=[C:25]([OH:2])[C:24]2=4)[NH:14][CH2:15]3)[N:19]([CH3:35])[CH2:20]1)=[O:34])[CH3:33]

Participants

Reactant 2

HCID 7416Nitrobenzene

HCID 131716087HCID 131716087, compound

Product 1

HCID 131716086HCID 131716086, compound

Procedure

With nitrobenzene and 3-(13-bromo-1-tert-butyldimethylsilyl-2,3-dihydro-6-methyl-8α-ergolinyl)-1,1-diethylurea:

Sources & evidence

ORD record: ord-2f6480d1c386487bb32afe15a2d8f0fc
Source dataset: uspto-grants-1989_09
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04863929

Reaction notes

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