Nitrobenzene → HCID 131716088, compound

HRID 1607067Notes

Reaction equation

[N+](C1C=CC=CC=1)([O-])=[O:2].Br[C:11]1[CH:12]=[C:13]2[C:26]3[C:16]([CH2:17][C@@H:18]4[C@@H:23]([C:24]=3[CH:25]=1)[CH2:22][C@H:21]([NH:27][C:28](=[O:34])[N:29]([CH2:32][CH3:33])[CH2:30][CH3:31])[CH2:20][N:19]4[CH2:35]CC)=[CH:15][N:14]2[Si](C(C)(C)C)(C)C>>[CH2:30]([N:29]([CH2:32][CH3:33])[C:28]([NH:27][C@H:21]1[CH2:22][C@H:23]2[C@@H:18]([CH2:17][CH:16]3[C:26]4[C:13](=[CH:12][C:11]([OH:2])=[CH:25][C:24]2=4)[NH:14][CH2:15]3)[N:19]([CH3:35])[CH2:20]1)=[O:34])[CH3:31]

Participants

Reactant 2

HCID 7416Nitrobenzene

HCID 131716089HCID 131716089, compound

Product 1

HCID 131716088HCID 131716088, compound

Procedure

With nitrobenzene and 3-(13-bromo-1-tert-butyldimethylsilyl-6-n-propyl-8α-ergolinyl)-1,1-diethylurea:

Sources & evidence

ORD record: ord-9ddf945f527b4f6bb4f8fa9f5b49473a
Source dataset: uspto-grants-1989_09
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04863929

Reaction notes

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