Iodine → HCID 131716100, compound

HRID 1607078Notes

Reaction equation

HRID 1607078 reaction equation
[I:1]I.Br[C:4]1[CH:5]=[C:6]2[C:19]3[C:9]([CH2:10][C@@H:11]4[C@@H:16]([C:17]=3[CH:18]=1)[CH2:15][C@H:14]([NH:20][C:21](=[O:27])[N:22]([CH2:25][CH3:26])[CH2:23][CH3:24])[CH2:13][N:12]4[CH2:28]CC)=[CH:8][N:7]2[Si](C(C)(C)C)(C)C>>[I:1][C:18]1[C:17]2=[C:19]3[C:6]([NH:7][CH:8]=[C:9]3[CH2:10][C@@H:11]3[C:16]2=[CH:15][C@H:14]([NH:20][C:21](=[O:27])[N:22]([CH2:25][CH3:26])[CH2:23][CH3:24])[CH2:13][N:12]3[CH3:28])=[CH:5][CH:4]=1

Participants

3

Reactant 2

HCID 807IodineHCID 131716089HCID 131716089, compound

Product 1

HCID 131716100HCID 131716100, compound

Procedure

With iodine and 3-(13-bromo-1-tert-butyldimethylsilyl-6-n-propyl-8α-ergolinyl)-1,1-diethylurea:

Sources & evidence

ORD record
ord-03e1a580a1c048449cae908dc8779fb3
Source dataset
uspto-grants-1989_09
Patent number
US04863929

Reaction notes

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