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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1607159Generated: October 30, 2026

HCID 19851967, compound → 3-[3-(4-Acetyl-3-methoxy-2-n-propylphenoxy)-propoxy]-aniline

https://huagongshe.com/reaction/1607159

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 19851967HCID 19851967—
CatalystNickelHCID 935—
SolventTetrahydrofuranHCID 8028—
Product3-[3-(4-Acetyl-3-methoxy-2-n-propylphenoxy)-propoxy]-anilineHCID 19851940—

Reaction Steps

2.0 g of Raney nickel are added to a solution of 10 g of 3-[3-(4-acetyl-3-methoxy-2-n-propylphenoxy)-propoxy]-nitrobenzene in 100 ml of tetrahydrofuran and the whole is hydrogenated at room temperature. The catalyst is filtered off and washed with tetrahydrofuran. After concentration of the filtrate by evaporation under reduced pressure, 3-[3-(4-acetyl-3-methoxy-2-n-propylphenoxy)-propoxy]-aniline is obtained in the form of a colourless oil.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04863942
Source datasetuspto-grants-1989_09
ORD IDord-a71f4676f0e64491a36985df7bcfda98
Source noteuspto-grants-1989_09