HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 19851967, compound → 3-[3-(4-Acetyl-3-methoxy-2-n-propylphenoxy)-propoxy]-aniline
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 19851967 | HCID 19851967 | — |
| Catalyst | Nickel | HCID 935 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | 3-[3-(4-Acetyl-3-methoxy-2-n-propylphenoxy)-propoxy]-aniline | HCID 19851940 | — |
Reaction Steps
2.0 g of Raney nickel are added to a solution of 10 g of 3-[3-(4-acetyl-3-methoxy-2-n-propylphenoxy)-propoxy]-nitrobenzene in 100 ml of tetrahydrofuran and the whole is hydrogenated at room temperature. The catalyst is filtered off and washed with tetrahydrofuran. After concentration of the filtrate by evaporation under reduced pressure, 3-[3-(4-acetyl-3-methoxy-2-n-propylphenoxy)-propoxy]-aniline is obtained in the form of a colourless oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04863942 |
| Source dataset | uspto-grants-1989_09 |
| ORD ID | ord-a71f4676f0e64491a36985df7bcfda98 |
| Source note | uspto-grants-1989_09 |