HuagongsheHuagongshe Chemistry Print Report · For research reference only
Allyl bromide → HCID 19910733, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Allyl bromide | HCID 7841 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | HCID 14579764 | HCID 14579764 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | HCID 19910733 | HCID 19910733 | 118.3% |
Reaction Steps
A mixture of 2-ethyl 4 hydroxy 3 methylbenzofuran (760 mgs; 4.3mmoles), allyl bromide (1.0 g; 8.6 mmoles), anhydrous potassium carbonate (1.1 g; g; 8.6mmoles) 8.6mmoles) and acetone (50 ml) was refluxed for 4 hours. The mixture was filtered, concentrated, and chromatographed to obtain 1.1 g of the title compound as an oil which was used as such in the next step.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04863958 |
| Source dataset | uspto-grants-1989_09 |
| ORD ID | ord-ae8fc77c15f74e468e8881d99f504818 |
| Source note | uspto-grants-1989_09 |