HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-(p-Methoxybenzoyl)-3-methyl-4-hydroxy-5-allylbenzofuran → 2-(p-Methoxybenzyl)-3-methyl-4-hydroxy-5-propylbenzofuran
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-(p-Methoxybenzoyl)-3-methyl-4-hydroxy-5-allylbenzofuran | HCID 14579792 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 2-(p-Methoxybenzyl)-3-methyl-4-hydroxy-5-propylbenzofuran | HCID 14570889 | — |
Reaction Steps
A solution of 2-(p-methoxybenzoyl)-3-methyl-4-hydroxy-5-allylbenzofuran (40 mg) in ethanol (50 mL) was hydrogenated in a Parr hydrogenator in the presence of 10% palladium on charcoal at 40 psi. The catalyst was filtered and the filtrate was concentrated to dryness to yield 2-(p-methoxybenzyl)-3-methyl-4-hydroxy-5-propylbenzofuran, identical to the product prepared by the route described in Example 1.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04863958 |
| Source dataset | uspto-grants-1989_09 |
| ORD ID | ord-668f860e16334c93b87debd5baa4288d |
| Source note | uspto-grants-1989_09 |