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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1607284Generated: October 31, 2026

Carbonate Ion → HCID 14570912, compound

https://huagongshe.com/reaction/1607284

Reaction equation

Participants

RoleNameHCIDCharge
ReactantCarbonate IonHCID 19660—
ReactantHCID 14570911HCID 14570911—
SolventMethanolHCID 887—
SolventWaterHCID 962—
ProductHCID 14570912HCID 1457091279.7%

Reaction Steps

A solution of 2-(p-acetoxybenzyl)-3-methyl-4-acetoxy-5-propyl-7-chlorobenzofuran (150 mg, 0.36 mmole) in methanol (5 mL) and a saturated solution of ootassium carbonate (3 mL) was stirred at room temperature for 5 minutes. The reaction was poured in water, extracted with methylene chloride, washed with brine, dried (Na2SO4), and concentrated in vacuo to yield 107 mg (79%) of 2-(p-hydroxybenzyl)-3-methyl-4-acetoxy-5-propyl-7-chlorobenzofuran.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04863958
Source datasetuspto-grants-1989_09
ORD IDord-aa0192971c9b4fedac414e9259f2f629
Source noteuspto-grants-1989_09