HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenothrin → HCID 13105991, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenothrin | HCID 4767 | — |
| Reactant | Ozone | HCID 24823 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 13105991 | HCID 13105991 | — |
Reaction Steps
Ozone gas was bubbled at -78° C. into a solution of 3.50 g (10.0 mmol) of 3-phenoxyphenylmethyl 2,2-dimethyl- 3-(2-methyl-1-propenyl)cyclopropanecarboxylate obtained in Reference Example 2, in 20 ml of ethyl acetate. The subsequent operation was conducted in the same manner as those in Reference Example 5, whereby 2.66 g of 3-phenoxyphenylmethyl 2,2-dimethyl-3-formylcyclopropanecarboxylate was obtained as a colorless oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04864052 |
| Source dataset | uspto-grants-1989_09 |
| ORD ID | ord-ca4ee569229b4ec59683d6f7d225e6f6 |
| Source note | uspto-grants-1989_09 |