HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ozone → HCID 13318850, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ozone | HCID 24823 | — |
| Reactant | Cyphenothrin | HCID 38283 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 13318850 | HCID 13318850 | 72% |
Reaction Steps
Ozone gas was bubbled at -78° C. into a solution of 1.88 g (5.00 mmol) of cyano(3-phenoxyphenyl)methyl 2,2-dimethyl-3-(2-methyl-1-propenyl)cyclopropanecarboxylate obtained in Reference Example 3, in 10 ml of ethyl acetate. The subsequent operation was conducted in the same manner as in Reference Example 5, whereby 1.26 g of cyano(3-phenoxyphenyl)methyl 2,2-dimethyl-3-formylcyclopropanecarboxylate was obtained as a colorless oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04864052 |
| Source dataset | uspto-grants-1989_09 |
| ORD ID | ord-8d525ff3d1e84a98bd21575f98d3e7e8 |
| Source note | uspto-grants-1989_09 |