HRID1607396

反应详情

EQUATION

反应方程式

HRID 1607396 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

A solution of 2.0 g of 3-ethoxycarbonyl-4-(1-naphthyl)-3-butenoic acid in 100 ml of acetic acid was hydrogenated over 900 mg of a 10% palladium/charcoal under a hydrogen atmosphere at room temperature. After filtration of the catalyst, the reaction solution was concentrated under reduced pressure to obtain 1.46 g of 3-ethoxycarbonyl-4-(1-naphthyl)butyric acid as a brown oil.

WORKUP

后处理

  1. filtrationAfter filtration of the catalyst
  2. concentrationthe reaction solution was concentrated under reduced pressure