HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonium Hydroxide → HCID 14547363, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonium Hydroxide | HCID 14923 | — |
| Reactant | HCID 14547360 | HCID 14547360 | — |
| Solvent | Sulfuric Acid | HCID 1118 | — |
| Product | HCID 14547363 | HCID 14547363 | 52.9% |
Reaction Steps
1-(2-Phenoxyethyl)-4-benzyl-2-hydroxy-6-oxopiperazine (4 g) was added to concentrated sulphuric acid (50 ml) at 0°-10° and the mixture stirred for 30 min. The resulting solution was poured onto ice, basified with NH4OH and extracted with chloroform to give the title compound as a pale oil (2 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04866056 |
| Source dataset | uspto-grants-1989_09 |
| ORD ID | ord-b9ef64c427e446848aa040a9e8355570 |
| Source note | uspto-grants-1989_09 |