HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl chloroformate → HCID 23052455, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl chloroformate | HCID 10928 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | HCID 5148089 | HCID 5148089 | — |
| Solvent | 1,1,1-Trichloroethane | HCID 6278 | — |
| Product | HCID 23052455 | HCID 23052455 | — |
Reaction Steps
A mixture of 3 (23.9 g, 0.2 mol), ethyl chloroformate (25 g, 0.23 mol) and potassium carbonate (30 g, 0.22 mol) in 1,1,1-trichloroethane (200 ml) was refluxed overnight.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04866077 |
| Source dataset | uspto-grants-1989_09 |
| ORD ID | ord-03f38ec6cea2414ca70fb150e83625b5 |
| Source note | uspto-grants-1989_09 |