1-Chloro-4-nitrobenzene → HCID 14305464, compound

Participants

Reaction Steps

A mixture of 2'-(2,4-difluorophenoxy)-4'-mercaptomethanesulfonanilide (1.5 g), p-chloronitrobenzene (0.75 g) and potassium carbonate (0.66 g) in xylene (30 ml) was stirred and refluxed for 5 hours. The reaction mixture was acidified, washed with water, dried, and concentrated to dryness. The residual oil was crystallized from ethanol to give crystals of 2'-(2,4-difluorophenoxy)-4'-(4-nitrophenylthio)methanesulfonanilide (1.5 g).

Provenance & Evidence