HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 19785761, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | Methacryloyl chloride | HCID 13528 | — |
| Reactant | 2-[2-(1,3-Dioxolan-2-yl)ethoxy]ethan-1-ol | HCID 13070695 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 19785761 | HCID 19785761 | — |
Reaction Steps
The preparation was similar to that used for the preparation of the monomer designated III except that 22.0 g triethylamine, 32.4 g 2-[2(2-hydroxyethoxy)-ethyl]-1,3-dioxolane and 180 ml methylene chloride were added initially and 23.22 g methacryloyl chloride were added dropwise. The monomer was purified by distillation at 106° C. under 0.2 mm Hg pressure.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04866151 |
| Source dataset | uspto-grants-1989_09 |
| ORD ID | ord-fd1685f52a3f49e99a4ea28615699047 |
| Source note | uspto-grants-1989_09 |