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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1607782Generated: October 25, 2026

m-Chloroperbenzoic acid → 4-(4,5-Epoxypentoxy)-4'-nitrobiphenyl

https://huagongshe.com/reaction/1607782

Reaction equation

Participants

RoleNameHCIDCharge
Reactantm-Chloroperbenzoic acidHCID 70297—
Reactant4-(4-Pentenoxy)-4'-nitrobiphenylHCID 19901284—
SolventDichloromethaneHCID 6344—
Product4-(4,5-Epoxypentoxy)-4'-nitrobiphenylHCID 22163019—

Reaction Conditions

Temperature0 °C

Reaction Steps

To 250 ml of methylene chloride is added 28.3 g of 4-(4-penteneoxy)-4'-nitrobiphenyl. The solution is cooled to 0° C.,and 18 g of meta-chloroperbenzoic acid is added slowly. The mixture is stirred at 0° C. for 24 hours, and allowed to warm to room temperature.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04867538
Source datasetuspto-grants-1989_09
ORD IDord-0512e8fd2ffb448cb418893863e87e58
Source noteuspto-grants-1989_09