Sodium Methoxide → 16-(p-Methylphenoxy)-hexadeca-5,8,11,14-tetraynoic acid sodium salt

HRID 1607823Notes

Reaction equation

HRID 1607823 reaction equation
C[O-].[Na+:3].[CH3:4][C:5]1[CH:29]=[CH:28][C:8]([O:9][CH2:10][C:11]#[C:12][CH2:13][C:14]#[C:15][CH2:16][C:17]#[C:18][CH2:19][C:20]#[C:21][CH2:22][CH2:23][CH2:24][C:25]([OH:27])=[O:26])=[CH:7][CH:6]=1>CO>[Na+:3].[CH3:4][C:5]1[CH:29]=[CH:28][C:8]([O:9][CH2:10][C:11]#[C:12][CH2:13][C:14]#[C:15][CH2:16][C:17]#[C:18][CH2:19][C:20]#[C:21][CH2:22][CH2:23][CH2:24][C:25]([O-:27])=[O:26])=[CH:7][CH:6]=1

Participants

4

Reactant 2

HCID 10942334Sodium MethoxideHCID 1457896816-(p-Methylphenoxy)hexadeca-5,8,11,14-tetraynoic acid

Product 1

HCID 7039575816-(p-Methylphenoxy)-hexadeca-5,8,11,14-tetraynoic acid sodium salt

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

Sodium methoxide (82 mg) is added to a solution of 16-(p-methylphenoxy)-hexadeca-5,8,11,14-tetraynoic acid (500 mg) in methanol (5 ml). The solution is then evaporated to dryness to afford 16-(p-methylphenoxy)-hexadeca-5,8,11,14-tetraynoic acid sodium salt.

Workup

  1. customThe solution is then evaporated to dryness

Sources & evidence

ORD record
ord-6059bce79eca4d309861e9bd13de13a2
Source dataset
uspto-grants-1989_09
Patent number
US04867915

Reaction notes

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