HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Hydroxybenzaldehyde → 4-(2-quinolinylmethoxy)Benzaldehyde
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Hydroxybenzaldehyde | HCID 126 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 2-(Chloromethyl)quinoline hydrochloride | HCID 3083823 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | 4-(2-quinolinylmethoxy)Benzaldehyde | HCID 14578960 | — |
Reaction Steps
From a mixture of 4-hydroxybenzaldehyde (5 g), 2-chloromethylquinoline hydrochloride (10.8 g) and anhydrous potassium carbonate (80 g) in dimethylformamide (100 ml), a total of 6.6 grams of captioned product as an off-white colored solid, m.p. 69°-72° C., was prepared similarily as in Example 1A.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04868193 |
| Source dataset | uspto-grants-1989_09 |
| ORD ID | ord-3618b39659d846049b3890845610d1d9 |
| Source note | uspto-grants-1989_09 |