HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanol → HCID 14065925, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | HCID 14438342 | HCID 14438342 | — |
| Product | HCID 14065925 | HCID 14065925 | — |
Reaction Steps
[R]-(-)-9-chloro-3-methyl-5-nonyn-4-one was prepared by the method of Example 35 from sec-butyl(5-chloro-1-pentynyl)isopropoxyborane. [α]75D -12.84 (c 1.89, MeOH); IR (neat) 2213, 1671 cm1. 13C NMR (CDCl3) δ191.9, 92.2, 80.5, 50.0, 43.2, 30.5, 25.8, 16.4, 15.5, 11.4. MS m/e % (chemical ionization) 187 (100).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04868337 |
| Source dataset | uspto-grants-1989_09 |
| ORD ID | ord-52b1b23d27b24559ba7101f844b23642 |
| Source note | uspto-grants-1989_09 |