HuagongsheHuagongshe Chemistry Print Report · For research reference only
Aniline → HCID 14626975, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Aniline | HCID 6115 | — |
| Reactant | 3-Chloro-4,5-dipropargyloxybenzaldehyde | HCID 14130305 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | HCID 14626975 | HCID 14626975 | 101.1% |
Reaction Steps
A mixture of 3-chloro-4,5-dipropargyloxybenzaldehyde (1.00 g) and aniline (0.37 g) in benzene (30 ml) was stirred under reflux for 3 hours, followed by concentration under reduced pressure to give N-(3-chloro-4,5-dipropargyloxybenzyliden)aniline (1.30 g). nD23.0 1.5890.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04870064 |
| Source dataset | uspto-grants-1989_09 |
| ORD ID | ord-bb1042df84c648d58ede17c8c4ea2604 |
| Source note | uspto-grants-1989_09 |