HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 13592262, compound → HCID 13592278, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 13592262 | HCID 13592262 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 13592278 | HCID 13592278 | 98% |
Reaction Steps
A mixture of 1.95 g of the 5,5-bis(azidomethyl)-1,3-dioxane, 0.5 g of 10% palladium on calcium carbonate and 40 ml of ethanol was reduced for 2 hours and then filtered. The filtrate was evaporated, giving 1.41 g of 1,3-dioxane-5,5-dimethanamine as an oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04870070 |
| Source dataset | uspto-grants-1989_09 |
| ORD ID | ord-df7829e226764194b63132505f78a339 |
| Source note | uspto-grants-1989_09 |